EQUIPMENT
CHEMISTRY LABORATORY
Chemical laboratory benches and hoods
Apparatus for the synthesis of materials
Balances
Centrifuge
The optical microscope
Rolling thin film ovens (RTFOT) sistema di invecchiamento bitume;
Instrumentation for the realization of macro and micro emulsions
NMR spectroscopy
Bruker NMR spectrometer AVANCE 300 Wide Bore
High Resolution probe: BBO 5mm multinuclear probe with Deuterium lock. Temperature range: -150°C /+180°C.
Diffusion probe: Diff30 Z-diff using 30 G/cm/A multinuclear with substitutable inserts of 5 mm (1H, 19F, 7Li, 31P, 2H, 27Al, 13C, ect.). Gradient strengths up to 1200 G/cm. Temperature range: -100°C / 200°C.
Micro-Imaging probe: probe for MRI with 3 substitutable RF inserts on 1H at different diameter (4, 15 and 25 mm).
Rheo-NMR probe: probe for MRI under shear.
Magic Angle Spinning (MAS) probe
DYNAMIC MECHANICAL ANALYSIS
DMA 25 – Acoem/Metravib
ASSETS
Force: from low levels (+/-0.001N) up to high forces (+/-25 Newtons for DMA25)
DMA25 maximum force expandable to +/-50 Newtons for rigid materials or large specimens
Displacement: from +/-1µm to +/-3mm
Frequency: from 0.00001 Hz to 200 Hz
Temperature: from -150°C to 500°C
Multi-purpose thermal chamber with window, allowing for gas atmosphere
Flexible and user-friendly Dynatest software including advanced control algorithms
APPLICATIONS
DMA and TMA testing
Determination of glass and secondary transitions
Static and quasi static testing: creep, stress relaxation, tension, compression, etc.
Particularly well suited to polymer and composite characterization
Impedance Spectroscopy
Autolab PGSTAT 30 with FRA2 module (Ecochemie):
Potentiostat/Galvanostat Autolab PGSTAT 30 with FRA2 module (Ecochemie):
maximum output voltage: +/- 30 V;
maximum output current: +/- 1 A;
current resolution: 30 fA on the 10 nA current range;
potentiostat bandwith: > 1 Mhz;
frequency range: 10 µHz to 1 MHz.
Among various cells, there is a home-made conductivity cell for measurements on solid samples (powders, membranes, gels), with temperature control.
Fuel Cell test
BEKKTECH BT-112 Cell / Humidification system (Fuel Cell Technologies)
Beckktech Model BT-112 In Plane Conductivity Cell for 5 cm2 Cell
Model 5SCH, Single Cell Hardware Assembly
Equipment for conductivity measurements and testing on polymeric membrane fuel cells (PEMFC);
Humidification system (Fuel Cell Technologies, Inc., Albuquerque, NM, USA)
Rheometer RFS-III
Shear-strain controlled
Strain controlled rheometer equipped with several geometries ( plate plate, cone plate, couette, double couette, micro couette). Temperature is controlled by a water circulator apparatus or Peltier system according the the used geometry (-30°C to +150°C ± 0.1°C ).
Motor: High Performance LS ;
Angular Velocity Range: 2x10-6 - 200 rad/s ;
Strain Amplitude: 5 µrad - 500 mrad;
Angular Frequency: 10-5 - 500 rad/s;
Torque Range: 2 µN.m - 200 mN.m;
Normal/Axial Force Range: 0.002 - 20 N ;
Peltier Plate: -30 to 150 °C ;
Bath: -10 to 150 °C.
Rheometer SR-5000
Shear-stress controlled
Stress-controlled rheometer DSR5000 (Rheometrics Scientific, USA) equipped with several geometries ( plate plate, cone plate, couette). Temperature is controlled by water circulator apparatus or Peltier system according the the used geometry (-30°C to +150°C ± 0.1°C ).
Measurements: stress – controlled measurements;
Max. Frequency ω [rad/s]: 500;
Stress range [Pa]: 0,3 - 1000 ;
Torque [mNm]: 0,001 - 20 ;
Phase angle [μrad]: 5 x 10-4 - 5 x 106 ;
Temperature range [°C]: 35 – 350 ;
Software: RSI Orchestrator .
DSC and micro-DSC
Setaram-131
Temperature range: Ambient to 700 °C ;
With cooling accessories : -170 °C to 500 °C (Liquid Nitrogen Accessory) ;
Cooling time : 12 min (500 °C to 100 °C) Air - 12 min (25 °C to -100 °C) Liquid Nitrogen Accessory ;
RMS Noise (200°C) : 1.5 µW ;
Time constant : 3s;
Gases : included gas switch from gas A to gas B ;
Dimensions (Height / Width / Depth): 40 / 53 / 58 cm (15.7 / 20.9 / 22.8 in);
Power requirements : 230 V – 50/60 Hz.
Atomic absorption spectrometry
AA-6300 Atomic Absorption Spectrophotometer
High-throughput Dynamic Beam Management System
Ensures long-term stability with low noise level;
Provides the highest level of sensitivity for trace-level analysis (Direct determination -Flame: Pb, 0.1ppm; Furnace: Pb, 0.3ppb);
Dual-Detector System with Dual Background-Correction Function
Ensures maximum sensitivity and accurate background correction at all wavelengths;
Easy selection process provides optimum method for meeting analysis objectives;
Burner Height and Gas Flow Rates are Automatically Set for Each Element and Matrix
Ensures maximum sensitivity and superior detection limits;
Enables continuous measurement;
WizAArd Software - A Match for this Electronic Records Era
Manage user login ID names and passwords;
Manage authority restrictions according to user level;
Electronic signatures and audit trail functions have been equipped as standard;
Switch Smoothly Between Flame and Furnace - Without Tools
Comprehensive Flame Analysis
Highly Sensitive and Stable Flame Analysis
Comprehensive Furnace Analysis
Safe Furnace Mechanisms
Radon Detector
NanoReader
Type
PADC/CR-39 radon and thoron sensitive plastic material;
Typical background/transit track density value: 0.2 tracks per mm2;
Dimension
10x10x1mm at RSK type detector;
21x23x1mm at RSG type detector;
Extra feature: Double ID code, for both visual and automatic reading
PC interfacing: USB 2.0
Windows/Linux compatible